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muffle furnace

Lab Ash Furnace

Scope of application

It is used for carbon nanotube purification (removal of amorphous carbon impurities), ashing of ceramic precursors and residual carbon content testing of battery electrode materials.

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Lab Ash Furnace

An ashing furnace is a high-temperature heating device specifically designed for measuring the ash content of samples. It is a specialized application of a muffle furnace. It removes organic components from samples through high-temperature combustion, retaining the inorganic residue (ash). It is widely used in quality testing and analytical research in the food, chemical, environmental protection, coal, and pharmaceutical industries.

Lab Ash Furnace

Basic Working Principle
High-temperature oxidation principle: At a controlled temperature (typically 500-900°C), organic matter in the sample undergoes a complete oxidation reaction with oxygen, generating CO₂ and H₂O that volatilize, leaving behind inorganic salts and minerals.

Pyrolysis principle: Some samples undergo pyrolysis in the absence of oxygen, decomposing organic components into volatile substances and fixed carbon. Ultimately, the carbon is also oxidized and removed.

III. Main Components

  1. Furnace System
    Furnace Chamber Material: High-purity alumina ceramic fiber or polycrystalline mullite fiber, offering excellent high-temperature resistance (up to 1200°C)

Insulation: Multi-layer nanoporous insulation effectively reduces heat loss

Casing: Double-layer stainless steel with forced air cooling

  1. Heating System
    Heating Elements: High-quality resistance wire (nickel-chromium alloy) or silicon carbide rods

Heating Method: Surround heating to ensure temperature uniformity (within ±5°C)

Heating Rate: Programmable, up to 30°C/min

  1. Control System
    Temperature Controller: Utilizes PID intelligent control algorithm, with an accuracy of ±1°C

Human-Machine Interface: 7-inch color touch screen with multi-language support

Data Logging: Built-in memory can store 100 programs and supports USB export

  1. Safety Protection System
    Overtemperature Protection (dual thermocouple monitoring)

Overcurrent Protection

Automatic power off when furnace door is opened

Abnormal Alarm System

V. Classification of Ashing Furnaces

  1. Classification by Application
    Food Ashing Furnaces: Temperatures typically ≤ 600°C, complying with AOAC standards

Coal Ashing Furnaces: Temperatures up to 815°C, complying with ASTM standards

Pharmaceutical Ashing Furnaces: Equipped with precise weighing capabilities, complying with USP standards

Environmental Monitoring Ashing Furnaces: Used for atmospheric particulate matter analysis

  1. Classification by Heating Method
    Resistive Ashing Furnaces: Most common, with precise temperature control

Infrared Ashing Furnaces: Fast heating and energy-efficient

Microwave Ashing Furnaces: Short processing time, but expensive

VI. Typical Applications

  1. Food Industry
    Determination of Ash Content in Cereals and Flour (GB 5009.4)

Mineral Content Analysis of Dairy Products

Condiment Purity Testing

  1. Coal and Petroleum
    Determination of Coal Ash (GB/T 212)

Ash Analysis of Petroleum Coke (ASTM D4422)

  1. Pharmaceutical Industry
    Inspection of Residue on Ignition of APIs (Chinese Pharmacopoeia General Chapter 0841)

Determination of Heavy Metal Content in Traditional Chinese Medicines

  1. Environmental Monitoring
    Analysis of Atmospheric Particulate Matter (PM2.5/PM10) Composition

Sludge Incineration Residue Testing

VII. Operational Procedure (Taking Food Ash Content Determination as an Example)

Sample Preparation

Accurately weigh 2-5g of sample into a crucible that has been pre-ignited to a constant weight.

Pre-dry the sample.

Carbonization Stage

Place the crucible on an electric furnace and carbonize at low temperature until smoke is eliminated.

Ashing Stage

Transfer the crucible to an ashing furnace preheated to 525±25°C.

Maintain temperature until complete ashing (usually 2-4 hours).

Cool and weigh.

Remove and cool in a desiccator to room temperature.

Accurately weigh and calculate ash content.

Lab Ash Furnace Technical Parameters

ModelMax.temperatureInner volumeInner sizePower and Voltage
YX-1200-1L1200℃1L105*105*110mm1KW/AC220V
YX-1200-4.5L1200℃4.5L150*150*200mm2.5KW/AC220V
YX-1200-7.2L1200℃7.2L200*120*300mm3KW/AC220V
YX-1200-18L1200℃18L250*250*300mm5KW/AC220V
YX-1200-36L1200℃36L300*300*400mm9KW/AC380V
YX-1400-3.6L1400℃3.6L150*150*160mm4KW/AC220V
YX-1400-8L1400℃8L200*200*200mm6KW/AC220V
YX-1400-18L1400℃18L250*250*300mm9KW/AC220V

Lab Ash Furnace video

ash furnace

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