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hydrothermal autoclave reactor

hydrothermal autoclave reactor

Scope of application

The autoclave for hydrothermal synthesis is an indispensable tool for researchers engaged in nanomaterial synthesis, crystal growth, and chemical reaction studies.

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Hydrothermal autoclave reactor

A hydrothermal autoclave reactor is a high-pressure laboratory vessel designed for conducting chemical reactions under high temperature and pressure. It is mainly used in nanomaterial synthesis, crystal growth, and chemical compound preparation.

The autoclave consists of a stainless steel outer shell and an inner liner made of PTFE (Teflon) or PPL, providing superior corrosion resistance and thermal insulation. Its design ensures safety, chemical purity, and consistent reaction results in laboratory environments.

hydrothermal autoclave reactor

Working Principle of Hydrothermal Autoclave

The hydrothermal autoclave operates by creating a closed, high-pressure environment. A solution containing reactants is placed inside the Teflon liner, sealed within the stainless steel chamber, and heated in an oven. As the temperature rises, vapor pressure builds up, promoting the formation of crystals, nanoparticles, or composite materials that cannot be produced under normal conditions.

This method—known as hydrothermal synthesis—is essential for materials science, chemistry, and nanotechnology research.


Key Features of Hydrothermal Autoclave Reactor

  • High Temperature Resistance: Can operate safely up to 280°C.
  • Pressure Endurance: Withstands up to 3 MPa internal pressure.
  • Corrosion-Resistant Interior: PTFE liner ensures a contamination-free environment.
  • Stainless Steel Durability: Provides mechanical strength and safety.
  • Leak-Proof Design: Precision threading and sealing prevent leakage.
  • Multiple Capacities: Available in 25 mL, 50 mL, 100 mL, 200 mL, and 500 mL volumes.

Applications of Hydrothermal Autoclave Reactor

The hydrothermal autoclave reactor is widely used across multiple industries and research areas:

  • Nanomaterial Synthesis: e.g., ZnO, TiO₂, Fe₃O₄ nanoparticles.
  • Crystal and Ceramic Growth: Used for zeolites, perovskites, and mineral samples.
  • Catalyst Preparation: Helps form high-purity catalyst materials.
  • Geochemical Research: Studies mineral formation under geological conditions.
  • Pharmaceutical and Chemical Synthesis: Produces organic and inorganic compounds.

How to Use a Hydrothermal Autoclave

  1. Place your sample and solvent inside the PTFE liner.
  2. Seal the liner and insert it into the stainless steel outer vessel.
  3. Tighten the lid with the provided wrench or thread lock.
  4. Heat the autoclave in an oven or furnace at the target temperature.
  5. Allow it to cool naturally after reaction completion.
  6. Open the vessel carefully and clean the liner thoroughly.

Safety Guidelines

  • Never exceed the rated temperature or pressure.
  • Avoid quick cooling or sudden depressurization.
  • Use gloves and protective eyewear when handling.
  • Regularly inspect the gasket and sealing components.
  • Clean and dry the reactor after every use.

Advantages of Hydrothermal Autoclave Reactor

Long service life with minimal maintenance.

Ensures high-purity experimental results.

Safe and durable dual-layer design.

Compatible with hydrothermal and solvothermal synthesis.

Compact and convenient for laboratory operation.

ModelVolume(mL)pressure(MPa)temperature(℃)Lining material(PTFE)
YHHW-5PTFE53220polytetrafluoroethylene
YHHW-10PTFE103220polytetrafluoroethylene
YHHW-15PTFE153220polytetrafluoroethylene
YHHW-25PTFE253220polytetrafluoroethylene
YHHW-50PTFE503220polytetrafluoroethylene
YHHW-100PTFE1003220polytetrafluoroethylene
YHHW-150PTFE1503220polytetrafluoroethylene
YHHW-200PTFE2003220polytetrafluoroethylene
YHHW-250PTFE2503220polytetrafluoroethylene
YHHW-300PTFE3003220polytetrafluoroethylene
YHHW-400PTFE4003220polytetrafluoroethylene
YHHW-500PTFE5003220polytetrafluoroethylene
YHHW-1000PTFE10003220polytetrafluoroethylene
YHHW-1500PTFE15003220polytetrafluoroethylene
YHHW-2000PTFE20003220polytetrafluoroethylene
YHHW-2500PTFE25003220polytetrafluoroethylene
YHHW-3000PTFE30003220polytetrafluoroethylene
ModelVolume(mL)pressure(MPa)temperature(℃)Lining material(PPL)
YHHB-5PPL53300Para-polyphenylene
YHHB-10PPL103300Para-polyphenylene
YHHB-15PPL153300Para-polyphenylene
YHHB-25PPL253300Para-polyphenylene
YHHB-50PPL503300Para-polyphenylene
YHHB-100PPL1003300Para-polyphenylene
YHHB-150PPL1503300Para-polyphenylene
YHHB-200PPL2003300Para-polyphenylene
YHHB-250PPL2503300Para-polyphenylene
YHHB-300PPL3003300Para-polyphenylene
YHHB-400PPL4003300Para-polyphenylene
YHHB-500PPL5003300Para-polyphenylene
YHHB-1000PPL10003300Para-polyphenylene

Hydrothermal autoclave video

hydrothermal autoclave

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